Asif Ur Rehman, Pedro Navarrete-Segado, Metin U. Salamci, Christine Frances, Mallorie Tourbin and David Grossin
The consolidation process and morphology evolution in ceramics-based additive manufacturing (AM) are still not well-understood. As a way to better understand the ceramic selective…
Abstract
Purpose
The consolidation process and morphology evolution in ceramics-based additive manufacturing (AM) are still not well-understood. As a way to better understand the ceramic selective laser sintering (SLS), a dynamic three-dimensional computational model was developed to forecast thermal behavior of hydroxyapatite (HA) bioceramic.
Design/methodology/approach
AM has revolutionized automotive, biomedical and aerospace industries, among many others. AM provides design and geometric freedom, rapid product customization and manufacturing flexibility through its layer-by-layer technique. However, a very limited number of materials are printable because of rapid melting and solidification hysteresis. Melting-solidification dynamics in powder bed fusion are usually correlated with welding, often ignoring the intrinsic properties of the laser irradiation; unsurprisingly, the printable materials are mostly the well-known weldable materials.
Findings
The consolidation mechanism of HA was identified during its processing in a ceramic SLS device, then the effect of the laser energy density was studied to see how it affects the processing window. Premature sintering and sintering regimes were revealed and elaborated in detail. The full consolidation beyond sintering was also revealed along with its interaction to baseplate.
Originality/value
These findings provide important insight into the consolidation mechanism of HA ceramics, which will be the cornerstone for extending the range of materials in laser powder bed fusion of ceramics.
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Muhammad Arif Mahmood, Andrei C. Popescu, Mihai Oane, Carmen Ristoscu and Ion N. Mihailescu
This paper aims to develop efficient and simple models for thermal distribution, melt pool dimensions and controlled phase change in the laser additive manufacturing (AM) of bulk…
Abstract
Purpose
This paper aims to develop efficient and simple models for thermal distribution, melt pool dimensions and controlled phase change in the laser additive manufacturing (AM) of bulk and powder particles ceramic materials.
Design/methodology/approach
This paper proposes new analytical models for the AM of bulk and powder bed ceramic materials. A volumetric moving heat source, along with the complete melting of bulk and powder particle materials, is taken into account. Different values of laser absorption coefficient in solid and liquid states have been used to investigate the phase transformation. Furthermore, the pores and voids dimensions are also included in the modeling. Theoretical predictions have been compared with the experimental analyses and finite element simulations in laser to silicon nitride and laser to alumina interaction. The analysis focuses on the impact of laser power and scanning speed on the melt pool width and depth evolution into the bulk substrate and powder bed.
Findings
This study shows that the powder particles exhibit a higher thermal distribution value than the bulk substrate because of voids in the powder layer. The laser beam experiences multiple reflections in the presence of porosity/voids, thus increasing the surface absorption coefficient, which becomes relevant with the increment in the pore/void dimension. A direct relationship has been found between the laser power and melt pool dimensions, while the scanning speed displayed an inverse relationship for the melt pool width and length. Larger melt dimensions were inferred in the case of laser–powder particle interaction compared with laser–bulk substrate interaction. A close correlation was found between the analytical simulations, experimental investigations and numerical simulation results within the range of 4%–8%.
Originality/value
This paper fulfills an identified need to develop efficient and simplified models for ceramics laser AM by taking into account different laser absorption coefficients in solid and liquid form, voids and pores dimensions and controlled phase transformation to avoid vapors and plasma formation. The limitation of the finite element simulation model is that the solution is strongly dependent on the mesh quality and accuracy directly linked to the computation efficiency and time. A finer mesh requires a longer computing time than a coarse mesh. Finite element simulations require, however, specialized skills.
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Swee Leong Sing, Wai Yee Yeong, Florencia Edith Wiria, Bee Yen Tay, Ziqiang Zhao, Lin Zhao, Zhiling Tian and Shoufeng Yang
This paper aims to provide a review on the process of additive manufacturing of ceramic materials, focusing on partial and full melting of ceramic powder by a high-energy laser…
Abstract
Purpose
This paper aims to provide a review on the process of additive manufacturing of ceramic materials, focusing on partial and full melting of ceramic powder by a high-energy laser beam without the use of binders.
Design/methodology/approach
Selective laser sintering or melting (SLS/SLM) techniques are first introduced, followed by analysis of results from silica (SiO2), zirconia (ZrO2) and ceramic-reinforced metal matrix composites processed by direct laser sintering and melting.
Findings
At the current state of technology, it is still a challenge to fabricate dense ceramic components directly using SLS/SLM. Critical challenges encountered during direct laser melting of ceramic will be discussed, including deposition of ceramic powder layer, interaction between laser and powder particles, dynamic melting and consolidation mechanism of the process and the presence of residual stresses in ceramics processed via SLS/SLM.
Originality/value
Despite the challenges, SLS/SLM still has the potential in fabrication of ceramics. Additional research is needed to understand and establish the optimal interaction between the laser beam and ceramic powder bed for full density part fabrication. Looking into the future, other melting-based techniques for ceramic and composites are presented, along with their potential applications.
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Taylor Davis, Tracy W. Nelson and Nathan B. Crane
dding dopants to a powder bed could be a cost-effective method for spatially varying the material properties in laser powder bed fusion (LPBF) or for evaluating new materials and…
Abstract
Purpose
dding dopants to a powder bed could be a cost-effective method for spatially varying the material properties in laser powder bed fusion (LPBF) or for evaluating new materials and processing relationships. However, these additions may impact the selection of processing parameters. Furthermore, these impacts may be different when depositing nanoparticles into the powder bed than when the same composition is incorporated into the powder particles as by ball milling of powders or mixing similarly sized powders. This study aims to measure the changes in the single bead characteristics with laser power, laser scan speed, laser spot size and quantity of zirconia nanoparticle dopant added to SS 316 L powder.
Design/methodology/approach
A zirconia slurry was inkjet-printed into a single layer of 316 SS powder and dried. Single bead experiments were conducted on the composite powder. The line type (continuous vs balling) and the melt pool geometry were compared at various levels of zirconia doping.
Findings
The balling regime expands dramatically with the zirconia dopant to both higher and lower energy density values indicating the presence of multiple physical mechanisms that influence the resulting melt track morphology. However, the energy density required for continuous tracks was not impacted as significantly by zirconia addition. These results suggest that the addition of dopants may alter the process parameter ranges suitable for the fabrication of high-quality parts.
Originality/value
This work provides new insight into the potential impact of material doping on the ranges of energy density values that form continuous lines in single bead tests. It also illustrates a potential method for spatially varying material composition for process development or even part optimization in powder bed fusion without producing a mixed powder that cannot be recycled.
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Neal K. Vail, Badrinarayan Balasubramanian, Joel W. Barlow and Harris L. Marcus
Reports that measurable amounts of polymer degradation occur during the fabrication of objects from polymer coated ceramic powders by selective laser sintering (SLS). Argues that…
Abstract
Reports that measurable amounts of polymer degradation occur during the fabrication of objects from polymer coated ceramic powders by selective laser sintering (SLS). Argues that because the binder is important in achieving strong green parts that can be handled with minimal breakage during post‐processing operations, it is essential to minimize the extent of binder losses. As the first step towards understanding the mechanisms of binder degradation, this paper presents a thermal model of the physical system, noting that the agreement between theory and experiment are good. The model is used to help determine the most influential parameters affecting binder losses during fabrication from polymer coated powders. Predicts that adjustments to laser beam diameter, laser scanning distance and gaseous environment will strongly affect polymer binder degradation during processing. Further predicts correctly that polymer degradation during SLS processing is not sensitive to the inherent degradation kinetics of the polymer.
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Mahyar Khorasani, Ian Gibson, Amir Hossein Ghasemi, Elahe Hadavi and Bernard Rolfe
The purpose of this study is, to compare laser-based additive manufacturing and subtractive methods. Laser-based manufacturing is a widely used, noncontact, advanced manufacturing…
Abstract
Purpose
The purpose of this study is, to compare laser-based additive manufacturing and subtractive methods. Laser-based manufacturing is a widely used, noncontact, advanced manufacturing technique, which can be applied to a very wide range of materials, with particular emphasis on metals. In this paper, the governing principles of both laser-based subtractive of metals (LB-SM) and laser-based powder bed fusion (LB-PBF) of metallic materials are discussed and evaluated in terms of performance and capabilities. Using the principles of both laser-based methods, some new potential hybrid additive manufacturing options are discussed.
Design methodology approach
Production characteristics, such as surface quality, dimensional accuracy, material range, mechanical properties and applications, are reviewed and discussed. The process parameters for both LB-PBF and LB-SM were identified, and different factors that caused defects in both processes are explored. Advantages, disadvantages and limitations are explained and analyzed to shed light on the process selection for both additive and subtractive processes.
Findings
The performance of subtractive and additive processes is highly related to the material properties, such as diffusivity, reflectivity, thermal conductivity as well as laser parameters. LB-PBF has more influential factors affecting the quality of produced parts and is a more complex process. Both LB-SM and LB-PBF are flexible manufacturing methods that can be applied to a wide range of materials; however, they both suffer from low energy efficiency and production rate. These may be useful when producing highly innovative parts detailed, hollow products, such as medical implants.
Originality value
This paper reviews the literature for both LB-PBF and LB-SM; nevertheless, the main contributions of this paper are twofold. To the best of the authors’ knowledge, this paper is one of the first to discuss the effect of the production process (both additive and subtractive) on the quality of the produced components. Also, some options for the hybrid capability of both LB-PBF and LB-SM are suggested to produce complex components with the desired macro- and microscale features.
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Abid Ullah, HengAn Wu, Asif Ur Rehman, YinBo Zhu, Tingting Liu and Kai Zhang
The purpose of this paper is to eliminate Part defects and enrich additive manufacturing of ceramics. Laser powder bed fusion (L-PBF) experiments were carried to investigate the…
Abstract
Purpose
The purpose of this paper is to eliminate Part defects and enrich additive manufacturing of ceramics. Laser powder bed fusion (L-PBF) experiments were carried to investigate the effects of laser parameters and selective oxidation of Titanium (mixed with TiO2) on the microstructure, surface quality and melting state of Titania. The causes of several L-PBF parts defects were thoroughly analyzed.
Design/methodology/approach
Laser power and scanning speed were varied within a specific range (50–125 W and 170–200 mm/s, respectively). Furthermore, varying loads of Ti (1%, 3%, 5% and 15%) were mixed with TiO2, which was selectively oxidized with laser beam in the presence of oxygen environment.
Findings
Part defects such as cracks, pores and uneven grains growth were widely reduced in TiO2 L-PBF specimens. Increasing the laser power and decreasing the scanning speed shown significant improvements in the surface morphology of TiO2 ceramics. The amount of Ti material was fully melted and simultaneously changed into TiO2 by the application of the laser beam. The selective oxidation of Ti material also improved the melting condition, microstructure and surface quality of the specimens.
Originality/value
TiO2 ceramic specimens were produced through L-PBF process. Increasing the laser power and decreasing the scanning speed is an effective way to sufficiently melt the powders and reduce parts defects. Selective oxidation of Ti by a high power laser beam approach was used to improve the manufacturability of TiO2 specimens.
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Yaasin Abraham Mayi, Alexis Queva, Morgan Dal, Gildas Guillemot, Charlotte Metton, Clara Moriconi, Patrice Peyre and Michel Bellet
During thermal laser processes, heat transfer and fluid flow in the melt pool are primary driven by complex physical phenomena that take place at liquid/vapor interface. Hence…
Abstract
Purpose
During thermal laser processes, heat transfer and fluid flow in the melt pool are primary driven by complex physical phenomena that take place at liquid/vapor interface. Hence, the choice and setting of front description methods must be done carefully. Therefore, the purpose of this paper is to investigate to what extent front description methods may bias physical representativeness of numerical models of laser powder bed fusion (LPBF) process at melt pool scale.
Design/methodology/approach
Two multiphysical LPBF models are confronted: a Level-Set (LS) front capturing model based on a C++ code and a front tracking model, developed with COMSOL Multiphysics® and based on Arbitrary Lagrangian–Eulerian (ALE) method. To do so, two minimal test cases of increasing complexity are defined. They are simplified to the largest degree, but they integrate multiphysics phenomena that are still relevant to LPBF process.
Findings
LS and ALE methods provide very similar descriptions of thermo-hydrodynamic phenomena that occur during LPBF, providing LS interface thickness is correctly calibrated and laser heat source is implemented with a modified continuum surface force formulation. With these calibrations, thermal predictions are identical. However, the velocity field in the LS model is systematically underestimated compared to the ALE approach, but the consequences on the predicted melt pool dimensions are minor.
Originality/value
This study fulfils the need for comprehensive methodology bases for modeling and calibrating multiphysical models of LPBF at melt pool scale. This paper also provides with reference data that may be used by any researcher willing to verify their own numerical method.
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Mehrshad Mehrpouya, Daniel Tuma, Tom Vaneker, Mohamadreza Afrasiabi, Markus Bambach and Ian Gibson
This study aims to provide a comprehensive overview of the current state of the art in powder bed fusion (PBF) techniques for additive manufacturing of multiple materials. It…
Abstract
Purpose
This study aims to provide a comprehensive overview of the current state of the art in powder bed fusion (PBF) techniques for additive manufacturing of multiple materials. It reviews the emerging technologies in PBF multimaterial printing and summarizes the latest simulation approaches for modeling them. The topic of “multimaterial PBF techniques” is still very new, undeveloped, and of interest to academia and industry on many levels.
Design/methodology/approach
This is a review paper. The study approach was to carefully search for and investigate notable works and peer-reviewed publications concerning multimaterial three-dimensional printing using PBF techniques. The current methodologies, as well as their advantages and disadvantages, are cross-compared through a systematic review.
Findings
The results show that the development of multimaterial PBF techniques is still in its infancy as many fundamental “research” questions have yet to be addressed before production. Experimentation has many limitations and is costly; therefore, modeling and simulation can be very helpful and is, of course, possible; however, it is heavily dependent on the material data and computational power, so it needs further development in future studies.
Originality/value
This work investigates the multimaterial PBF techniques and discusses the novel printing methods with practical examples. Our literature survey revealed that the number of accounts on the predictive modeling of stresses and optimizing laser scan strategies in multimaterial PBF is low with a (very) limited range of applications. To facilitate future developments in this direction, the key information of the simulation efforts and the state-of-the-art computational models of multimaterial PBF are provided.
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Abid Ullah, Asif Ur Rehman, Metin Uymaz Salamci, Fatih Pıtır and Tingting Liu
This paper aims to reduce part defects and improve ceramic additive manufacturing (AM). Selective laser melting (SLM) experiments were carried out to explore the effect of laser…
Abstract
Purpose
This paper aims to reduce part defects and improve ceramic additive manufacturing (AM). Selective laser melting (SLM) experiments were carried out to explore the effect of laser power and scanning speed on the microstructure, melting behaviour and surface roughness of cuprous oxide (Cu2O) ceramic.
Design/methodology/approach
The experiments were designed based on varying laser power and scanning speed. The laser power was changed between 50 W and 140 W, and the scanning speed was changed between 170 mm/s and 210 mm/s. Other parameters, such as scanning strategy, layer thickness and hatch spacing, remain constant.
Findings
Laser power and scan speed are the two important laser parameters of great significance in the SLM technique that directly affect the molten state of ceramic powders. The findings reveal that Cu2O part defects are widely controlled by gradually increasing the laser power to 110 W and reducing the scanning speed to 170 mm/s. Furthermore, excessive laser power (>120 W) caused surface roughness, cavities and porous microstructure due to the extremely high energy input of the laser beam.
Originality/value
The SLM technique was used to produce Cu2O ceramic specimens. SLM of oxide ceramic became feasible using a slurry-based approach. The causes of several part defects such as spattering effect, crack initiation and propagation, the formation of porous microstructure, surface roughness and asymmetrical grain growth during the SLM of cuprous oxide (Cu2O) are thoroughly investigated.