Ewa Klimiec, Piotr Zachariasz, Halina Kaczmarek, Bogusław Królikowski and Sławomir Mackiewicz
This paper aims to present the details of isotactic polypropylene (it-PP) films with a cellular structure (air-cavities) dedicated to pressure sensors. The polymer composites…
Abstract
Purpose
This paper aims to present the details of isotactic polypropylene (it-PP) films with a cellular structure (air-cavities) dedicated to pressure sensors. The polymer composites (thin films enriched with 5 and 10 wt% of mineral fillers as Sillikolloid P 87 and glass beads) should exhibit suitable structural elasticity within specific stress ranges. After the deformation force is removed, the sensor material must completely restore its original shape and size.
Design/methodology/approach
Estimating the stiffness tensor element (C33) for polymer films (nonpolar space-charge electrets) by broadband resonance ultrasound spectroscopy is a relatively simple method of determining the safe stress range generated in thin pressure sensors. Therefore, ultrasonic and piezoelectric studies were carried out on four composite it-PP films. First, the longitudinal velocity (vL) of ultrasonic waves passing through the it-PP film in the z-direction (thickness) was evaluated from the ω-position of mechanical resonance of the so-called insertion loss function. In turn, the d33 coefficient was calculated from accumulated piezoelectric charge density response to mechanical stress.
Findings
Research is at an early stage; however, it can be seen that the mechanical orientation of the it-PP film improves its piezoelectric properties. Moreover, the three-year electric charge stability of the it-PP film seems promising.
Originality/value
Ultrasonic spectroscopy can be successfully handled as a validation method in the small-lot production of polymer films with the air-cavities structure intended for pressure sensors. The structural repeatability of polymer films is strongly related to a homogeneous distribution of the electric charge on the electret surface.
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Kyoo‐Seok Kim, Jae‐Pil Jung and Y. Norman Zhou
The aim of the paper is to study the feasibility of direct ultrasonic bonding between contact pad arrays on flexible printed circuit boards (FPCB) and rigid printed circuit boards…
Abstract
Purpose
The aim of the paper is to study the feasibility of direct ultrasonic bonding between contact pad arrays on flexible printed circuit boards (FPCB) and rigid printed circuit boards (RPCB) at ambient temperature.
Design/methodology/approach
Metallization layers on the RPCB comprised Sn on Cu while the pads on the FPCB consisted of Au/Ni/Cu. Prepared RPCB and FPCB were bonded by ultrasound at ambient temperature using an ultrasonic frequency of 20 kHz, a power of 1,400 W, and 0.62 MPa of bonding pressure. The bonded samples were cross‐sectioned and the joints and microstructures were observed by Field Emission Scanning Electron Microscopy (FE‐SEM) and Energy Dispersive Spectroscopy (EDS). The soundness of the joints was evaluated by pull testing.
Findings
Robust bonding between FPCB and RPCB was obtained by bonding for 1.0 and 1.5 s. This result has confirmed that direct room temperature ultrasonic bonding of Au and Sn is feasible. At a longer bonding time of 3.0 s, cracks and voids were found in the joints due to excessive ultrasonic energy. The IMC (intermetallic compound) between the Sn layer and pads of the RPCB was confirmed as Cu6Sn5. On the FPCB side, Cu6Sn5 and Ni3Sn4 were formed by contact with the facing Sn coating, and mechanically alloyed Cu0.81Ni0.19 was found within the pads. Meanwhile, the strength of bonded joints between FPCB and RPCB increased with bonding time up to 1.5 s and the maximum value reached 12.48 N. At 3.0 s bonding time, the strength decreased drastically, and showed 5.75 N. Footprints from the fracture surfaces showed that bonding started from the edges of the metal pads, and extended to the pad centers as ultrasonic bonding time was increased.
Originality/value
Direct ultrasonic bonding with transverse vibration at ambient temperature between the surface layers of the pads of FPCB and RPCB has been confirmed to be feasible.
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X.R. Zhang, L.Z. Liu, J.F. Li, W.W. Cui and L. Weng
The key purpose of this study was to investigate the effects of different ultrasonic irradiation times on the wettability and other properties of the resulting water-based…
Abstract
Purpose
The key purpose of this study was to investigate the effects of different ultrasonic irradiation times on the wettability and other properties of the resulting water-based coating. The subject water-based coating was prepared using water-soluble polyester and amino resins by ultrasonic oscillation.
Design/methodology/approach
The coating was prepared by polymerising polyester and amino resins in water using ultrasonic oscillation. The coating was baked for 40 seconds at 350°C to coalesce and solidify the film. The contact angle, thermal stability and mechanical properties of the film, as well as the molecular weight (MW) and structure of the polyester resin, were determined.
Findings
The contact angle of the coating was found to decrease with ultrasonic irradiation; the mechanical properties and thermal stability were not altered when the irradiation time was longer than 5 hours. The MW of the polyester initially decreased then increased and stabilized with ultrasonic irradiation. The structure of polyester molecule and aggregated state of the solidified coating were not changed by ultrasonic irradiation.
Research limitations/implications
In the study reported here, the effects of different ultrasonic irradiation times were investigated. Results of this research could benefit in-depth understanding of the influence of ultrasonic treatment on polyester resins and polyester coatings and could further promote the development of water-based coatings.
Originality/value
The contact angle of the water-based coating decreased by mechanical means. The effects of ultrasound on microstructure and properties of the coating and resin were discussed in detail.
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Seyed Foad Mousavi, Seyed Hassan Hashemabadi and Hossein Azizi Moghaddam
Invasive transit-time ultrasonic flow measurement involves the use of ultrasonic transducers, which sense the flowing fluid and are the most important parts of an ultrasonic…
Abstract
Purpose
Invasive transit-time ultrasonic flow measurement involves the use of ultrasonic transducers, which sense the flowing fluid and are the most important parts of an ultrasonic flowmeter. In this study, two ultrasonic transducers were designed, numerically simulated and fabricated to be used in an ultrasonic gas flowmeter.
Design/methodology/approach
PZT-5H piezoceramic elements with specific dimensions were designed and used as beating heart inside the transducers. Different methods, including impedance-frequency analysis, optical emission spectroscopy and performance tests in pressurized chambers were used to evaluate the piezoelectric elements, ultrasonic transducer housings and the fabricated transducers, respectively. In addition, finite element method results showed its ability for design stages of ultrasonic transducer.
Findings
Experimental results for transit time difference (TTD) and the normalized received voltage were compared with simulation results at the same conditions. There was a quite good agreement between the two method results. Extensive simulation results showed that under the considered range of environmental conditions, the change of acoustic path length has the most impact on TTD, with respect to temperature and pressure. A change of 1 mm in acoustic path length leads to 0.74 per cent change in TTD, approximately. In addition, for normalized received voltage, 1 bar change in pressure has the most impact and its value is as high as 3.76 per cent.
Practical implications
This method is possibly used in ultrasonic gas flowmeter fabrication.
Originality/value
In this work, design, fabrication, experimental tests and numerical simulation of ultrasonic transducers are presented.