K. Sivaprasad, V. Swarnalatha, V.V. Ravikumar and V. Muthupandi
The purpose of this paper is to study the corrosion behavior of as‐cryorolled and cryorolled‐short annealed commercially pure aluminum (CP‐Al) in 3.5 percent NaCl solution.
Abstract
Purpose
The purpose of this paper is to study the corrosion behavior of as‐cryorolled and cryorolled‐short annealed commercially pure aluminum (CP‐Al) in 3.5 percent NaCl solution.
Design/methodology/approach
Cast and homogenized CP‐Al samples are cryorolled from 7 to 0.7 mm at −80°C. Samples are short annealed at 125, 150 and 175°C for 3 min. Transmission electron microscope studies are performed to understand the effect of cryorolling and short annealing on microstructure. Corrosion behavior of these samples in 3.5 percent NaCl solution is evaluated by potentiodynamic polarization studies.
Findings
Though cryorolling adversely affects corrosion resistance of CP‐Al, short annealing can restore the loss in corrosion resistance partially by the recovery process. The extent of restoration of loss in corrosion resistance by short annealing is influenced by the texture.
Originality/value
The results obtained by this investigation help in understanding the effect of cryorolling and short annealing on corrosion behavior of CP‐Al.
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G. Yoganjaneyulu, V.V. Ravikumar and C. Sathiya Narayanan
The purpose of this paper is to investigate the strain distribution, stress-based fracture limit and corrosion behaviour of titanium Grade 2 sheets during single point incremental…
Abstract
Purpose
The purpose of this paper is to investigate the strain distribution, stress-based fracture limit and corrosion behaviour of titanium Grade 2 sheets during single point incremental forming (SPIF) process, with various computerized numerical control (CNC) spindle rotational speeds and step depths. The development of corrosion pits in 3.5 (%) NaCl solution has also been studied during the SPIF process.
Design/methodology/approach
A potentiodynamic polarization (PDP) study was performed to investigate the corrosion behaviour of titanium Grade 2 deformed samples, with various spindle rotational speeds in 3.5 (%) NaCl solution. The scanning electron microscope (SEM) and transmission electron microscope (TEM) analysis was carried out to study the fracture behaviour, dislocation densities and corrosion morphology of deformed samples.
Findings
The titanium Grade 2 sheets exhibited better strain distribution, fracture limit and corrosion resistance by increasing the CNC spindle rotational speeds, tool diameters and vertical step depths (VSD). It was recorded that varying the spindle speed affected plastic deformation which in turn affected corrosion rate.
Research limitations/implications
In this study, poor corrosion rate was observed for the as-received condition, and better corrosion rate was achieved at maximum speed of 600 rpm and 0.6 mm of VSD in the deformed sheet. This indicates that corrosion rate improved with increase in the plastic deformation. The EDS analysis report of corroded surface revealed the composition to be mainly of titanium and oxides.
Practical implications
This study discusses the strain distribution, stress-based fracture limit and corrosion behaviour by using titanium Grade 2 sheets during SPIF process.
Social implications
This study is useful in the field of automobile and industrial applications.
Originality/value
With an increase in the spindle rotational speeds and VSD, the titanium Grade 2 sheets showed better strain distribution, fracture limit and corrosion behaviour; the same is evidenced in fracture limit curve and PDP curves.
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G. Yoganjaneyulu, Y. Phaneendra, V.V. Ravikumar and C. Sathiya Narayanan
The purpose of this paper is to investigate the void coalescence and corrosion behaviour of titanium Grade 4 sheets during single point incremental forming (SPIF) process with…
Abstract
Purpose
The purpose of this paper is to investigate the void coalescence and corrosion behaviour of titanium Grade 4 sheets during single point incremental forming (SPIF) process with various spindle rotational speeds. The development of corrosion pits in 3.5 (%) NaCl solution has also been studied during SPIF process.
Design/methodology/approach
In this current research work, the void coalescence analysis and corrosion behaviour of titanium Grade 4 specimens were studied. A potentio-dynamic polarization (PDP) study was conducted to investigate the corrosion behaviour of titanium Grade 4 processed samples with various spindle speeds in 3.5 (%) NaCl solution. The scanning electron microscope and transmission electron microscope analysis was carried out to study the fracture behaviour and corrosion morphology of processed samples.
Findings
The titanium Grade 4 sheets obtained better formability and corrosion resistance by increasing the CNC spindle rotational speeds. In fact that, the significant plastic deformation affects the corrosion rate with various spindle speeds were recorded.
Originality/value
The spindle rotational speeds and vertical step depths increases then the titanium Grade 4 sheets showed better formability, void coalescence and corrosion behaviour as the same is evidenced in forming limit diagram and PDP curves.
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Girendra Kumar, Ashok Kumar and H.N. Bar
The purpose of this paper is to study the effect of mean stress and stress amplitude on the asymmetric cyclic deformation behavior of SA333 Gr-6 C-Mn steel. Such type of loading…
Abstract
Purpose
The purpose of this paper is to study the effect of mean stress and stress amplitude on the asymmetric cyclic deformation behavior of SA333 Gr-6 C-Mn steel. Such type of loading may arise during the service period because of the load fluctuations, thermal gradients and sudden loading like seismic events. Tests were also carried out at different temperatures to understand the effect of it on sensitiveness of the materials deformation behavior.
Design/methodology/approach
Cylindrical specimen of 8-mm gauge diameter and 15-mm gauge length was fabricated from the pipe section along its axis. Stress controlled ratcheting tests were carried out by using triangular waveform for cyclic loading. The strain accumulations were measured using 12.5-mm gauge length extensometer. Ratcheting tests were carried out at fixed stress amplitude of 400 MPa and mean stress varying from 0 to 75 MPa, whereas at the fixed mean stress of 100 MPa and stress amplitude varies from 300 to 400 MPa at 300°C. To study the effect of temperature on ratcheting behavior, tests were carried out at a load of 100 MPa mean stress and 350 MPa stress amplitude, with a varying temperature between room temperature and 350°C. The stress rate of 115 MPas-1 was kept constant for all the tests.
Findings
Increase in mean stress and stress amplitude, ratcheting strain and plastic strain amplitude increases, whereas ratcheting life decreases. With an increase in temperature, ratcheting life increases and strain accumulation decreases up to 300°C, whereas on further increase in temperature, strain accumulation increases with reduction in ratcheting life. Minimum ratcheting rate was observed at 250°C and 300°C. The dynamic strain aging (DSA) phenomena lead to the hardening of the material. The investigated steel shows DSA temperature regime lies between 250°C and 300°C. The failure modes at 250°C and 300°C temperature was transgranular, whereas at 350°C complete ductile.
Research limitations/implications
The stress rate and loading condition may vary to study the ratcheting behavior.
Practical implications
From this study, the critical cyclic load may be determined. The DSA temperature regime of this material is determined at this stress rate. This could help to evaluate the cyclic deformation behavior of the material with temperature changes.
Originality/value
In this investigation, the DSA temperature regime has been determined where maximum ratcheting life, minimum strain accumulation and ratcheting rate were observed. The critical load where the minimum life of the material occurred at elevated temperature is 100 MPa mean stress and 400 MPa stress amplitude.
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The purpose of this paper is to present the transmission and reflection characteristic of via holes in microwave planar circuits by the matrix‐penciled moment method (MP‐MOM…
Abstract
Purpose
The purpose of this paper is to present the transmission and reflection characteristic of via holes in microwave planar circuits by the matrix‐penciled moment method (MP‐MOM) including physical modeling, theoretical analysis, and experimental test. Especially, the experimental test is given in detail including device under test design, fixture design, and de‐embedding method.
Design/methodology/approach
The MP‐MOM is used to analyze the transmission and reflection characteristic of via holes in a wide frequency band. An emulator is built on MATLAB program (M‐file) to explore the effects of various parameters of via holes.
Findings
The smaller thickness of the dielectric‐slab means the more conductive to transfer. The smaller radius of the via hole means the more conducive to transfer. The lower dielectric constant means the more conductive to transfer.
Research limitations/implications
Some boundary conditions such as perfect magnetic conduction (PMC) and perfect electric condition have not been studied, and only perfectly matched layer, which means the infinite plane is dealt with.
Practical implications
The transmission and reflection characteristic of via holes will contribute to the design in such fields: microwave planar circuits, multilayer printed circuit boards, radio frequency integrated circuits, monolithic microwave integrated circuits, etc. which can guarantee the maximum transmission and the minimum reflection or radiation.
Originality/value
This paper presents the transmission and reflection characteristic of via holes with different parameters by the MP‐MOM and the design of experimental test including de‐embedding method.
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The purpose of this paper is to study the corrosion behaviour of Al-12Zn-3Mg-2.5Cu alloy by cast, precipitation hardening and non-isothermal step rolling cum cold/cryo rolling…
Abstract
Purpose
The purpose of this paper is to study the corrosion behaviour of Al-12Zn-3Mg-2.5Cu alloy by cast, precipitation hardening and non-isothermal step rolling cum cold/cryo rolling (−80 and −196°C) in 3.5 per cent NaCl solution.
Design/methodology/approach
Aluminium alloy with high alloying concentration (Zn: 12 per cent, Mg: 3 per cent, Cu: 2.5 per cent) was prepared by squeeze casting method with controlled process parameters. The cast alloy was solution treated at 450°C for 24 h and aged at 120°C with varying time intervals. Initially, the alloy also underwent non-isothermal step rolling from 6 mm to 3 mm at 400-100°C at the step of 100ºC with 15% reduction in thickness. Non-isothermal rolled alloy (3 mm thickness) was the starting material for further rolling at three different temperatures, such as room temperature, −80 and −190°C with 85 per cent reduction. Microstructural evolution during precipitation and thermo-mechanical processing was studied with the help of optical microscopy and electron microscopy. A potentio-dynamic polarization study was performed to evaluate the corrosion behaviour of Al-12Zn-3Mg-2.5Cu alloy processed in different conditions in 3.5 per cent NaCl solution.
Findings
There is a distinct evidence that the alloy exhibits varying corrosion resistance by changing its structural features. In fact, the alloy with ultra-fine grained structure exhibits good corrosion resistance than that of alloy in cast. This is attributed to a greater grain boundary region with high dislocation density, and plastic strain adversely affects the corrosion resistance.
Originality/value
The results obtained by this investigation help in understanding the effect of precipitation hardening and non-isothermal step rolling cum cold/cryo rolling (−80 and −196°C) on corrosion behaviour.
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Anasyida Abu Seman, Ji Kit Chan, Muhammad Anas Norazman, Zuhailawati Hussain, Dhindaw Brij and Azzura Ismail
This paper aims to investigate the corrosion behaviour of heat-treated and cryorolled Al 5052 alloys in different Cl− ion concentrations.
Abstract
Purpose
This paper aims to investigate the corrosion behaviour of heat-treated and cryorolled Al 5052 alloys in different Cl− ion concentrations.
Design/methodology/approach
NaCl solutions with concentrations of 0, 0.5, 3.5 and 5.5 per cent were selected. Samples were subjected to pre-heat treatment (annealing at 300 °C and solution treatment at 540 °C) and cryorolling up to 30 per cent reduction before undergoing corrosion tests. The corrosion behaviour of the samples was then investigated by potentiodynamic polarization. The microstructure of the corroded samples was evaluated under an optical microscope, and the percentages of pits on their surfaces were calculated.
Findings
The cryorolled samples had a lower corrosion rate than the samples that were not cryorolled. The cryorolled sample that underwent solution treatment showed the highest corrosion resistance among all the samples tested.
Practical implications
The commercial impact of the study is the possibility of using the cryorolled Al alloy in various ion chloride environment.
Originality/value
The obtained results help in understanding the corrosion behaviour of cryorolled samples under different heat treatment conditions.
Details
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Ajaya Kumar Panda and Swagatika Nanda
The purpose of this paper is to capture the pattern of return volatility and information spillover and the extent of conditional correlation among the stock markets of leading…
Abstract
Purpose
The purpose of this paper is to capture the pattern of return volatility and information spillover and the extent of conditional correlation among the stock markets of leading South American economies. It also examines the connectedness of market returns within the region.
Design/methodology/approach
The time series properties of weekly stock market returns of benchmark indices spanning from the second week of 1995 to the fourth week of December 2015 are analyzed. Using univariate auto-regressive conditional heteroscedastic, generalized auto-regressive conditional heteroscedastic, and dynamic conditional correlation multivariate GARCH model approaches, the study finds evidence of returns and volatility linkages along with the degree of connectedness among the markets.
Findings
The findings of this study are consistent with increasing market connectedness among a group of leading South American economies. Stocks exhibit relatively fewer asymmetries in conditional correlations in addition to conditional volatility; yet, the asymmetry is relatively less apparent in integrated markets. The results demonstrate that co-movements are higher toward the end of the sample period than in the early phase. The stock markets of Argentina, Brazil, Chile, and Peru are closely and strongly connected within the region followed by Colombia, whereas Venezuela is least connected with the group.
Practical implications
The implication is that foreign investors may benefit from the reduction of the risk by adding the stocks to their investment portfolio.
Originality/value
The unique features of the paper include a large sample of national stock returns with updated time series data set that reveals the time series properties and empirical evidence on volatility testing. Unlike other studies, this paper uncovers the relation between the stock markets within the same region facing the same market condition.
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Doğan Şimşek, Dursun Özyürek and Serdar Salman
The purpose of this study, the tribological behaviors at different temperatures of aluminium matrix composites (AMCs) with different amounts of ZrO2 added were investigated.
Abstract
Purpose
The purpose of this study, the tribological behaviors at different temperatures of aluminium matrix composites (AMCs) with different amounts of ZrO2 added were investigated.
Design/methodology/approach
Aluminium graphite (A356/2 wt% graphite (solid lubricant)) composite powders prepared by adding four different amounts (3 wt%, 6 wt%, 9 wt% and 12 wt%) of Zirconia (ZrO2) to the matrix were mechanically alloyed for 4 h. Wear tests were conducted at five different temperatures (20 °C, 100 °C, 180 °C, 260 °C and 340 °C) and for three different sliding distances (53 m, 72 m and 94 m) on the pin-on-disc type wear tester.
Findings
Results of the study showed that the highest hardness and density value were measured for 12% ZrO2 added AMC material. Wear test results showed that weight loss increases with increasing temperature; weight loss decreases at all temperatures with the increasing amount of reinforcement in the matrix.
Originality/value
In this paper, the tribological properties of aluminium matrix composites produced by the mechanical alloying method by adding different amounts of ZrO2 were determined by simulating the tribological properties at different loads and temperatures.
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Tushar Sonar, Visvalingam Balasubramanian, Sudersanan Malarvizhi, Thiruvenkatam Venkateswaran and Dhenuvakonda Sivakumar
The primary objective of this investigation is to optimize the constricted arc tungsten inert gas (CA-TIG) welding parameters specifically welding current (WC), arc constriction…
Abstract
Purpose
The primary objective of this investigation is to optimize the constricted arc tungsten inert gas (CA-TIG) welding parameters specifically welding current (WC), arc constriction current (ACC), ACC frequency (ACCF) and CA traverse speed to maximize the tensile properties of thin Inconel 718 sheets (2 mm thick) using a statistical technique of response surface methodology and desirability function for gas turbine engine applications.
Design/methodology/approach
The four factor – five level central composite design (4 × 5 – CCD) matrix pertaining to the minimum number of experiments was chosen in this investigation for designing the experimental matrix. The techniques of numerical and graphical optimization were used to find the optimal conditions of CA-TIG welding parameters.
Findings
The thin sheets of Inconel 718 (2 mm thick) can be welded successfully using CA-TIG welding process without any defects. The joints welded using optimized conditions of CA-TIG welding parameters showed maximum of 99.20%, 94.45% and 73.5% of base metal tensile strength, yield strength and elongation.
Originality/value
The joints made using optimized CA-TIG welding parameters disclosed 99.20% joint efficiency which is comparatively 20%–30% superior than conventional TIG welding process and comparable to costly electron beam welding and laser beam welding processes. The parametric mathematical equations were designed to predict the tensile properties of Inconel 718 joints accurately with a confidence level of 95% and less than 4.5% error. The mathematical relationships were also developed to predict the tensile properties of joints from the grain size (secondary dendritic arm spacing-SDAS) of fusion zone microstructure.