L.J. Golonka, M. Buczek, M. Hrovat, D. Belavič, A. Dziedzic, H. Roguszczak and T. Zawada
To find properties of screen printed PZT (PbZr0.53Ti0.47O3 with 6 per cent of PbO and 2 per cent of Pb5Ge3O11) thick films layers on LTCC substrate.
Abstract
Purpose
To find properties of screen printed PZT (PbZr0.53Ti0.47O3 with 6 per cent of PbO and 2 per cent of Pb5Ge3O11) thick films layers on LTCC substrate.
Design/methodology/approach
The influence of PZT firing time and electrode materials on electrical characteristics and microstructure were examined. A scanning electron microscope (SEM) equipped with an energy‐dispersive X‐ray (EDS) analyser was used for the microstructural and compositional analysis.
Findings
Microstructural and compositional analyses have shown the diffusion of SiO2 from LTCC into PZT layers and the diffusion of PbO in the opposite direction. SiO2 presumably forms low permitivity lead based silicates in PZT layer. The new phase deteriorates the piezoelectric properties. The amount of diffused materials was dependent upon the electrode material and increased with increasing firing time. Better properties, i.e. higher remanent polarisation and dielectric constant were achieved for samples with PdAg electrodes and shorter firing time.
Originality/value
New information on electrical and microstructural properties of thick film PZT made on LTCC substrate.
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Arkadiusz Dabrowski, Przemyslaw Rydygier, Mateusz Czok and Leszek Golonka
The purpose of this study was to design, fabricate and test devices based on transformers integrated with low-temperature co-fired ceramic (LTCC) modules with isolation between…
Abstract
Purpose
The purpose of this study was to design, fabricate and test devices based on transformers integrated with low-temperature co-fired ceramic (LTCC) modules with isolation between primary and secondary windings at the level between 6 and 12 kV.
Design/methodology/approach
Insulating properties of the LTCC were examined. Dielectric strength and volume resistivity were determined for common LTCC tapes: 951 (DuPont), 41020, 41060 (ESL), A6M (Ferro) and SK47 (KEKO). According to the determined properties, three different devices were designed, fabricated and tested: a compact DC/DC converter, a galvanic separator for serial digital bus and a transformer for high-voltage generator.
Findings
Breakdown field intensity higher than 40 kV/mm was obtained for the test samples set, whereas the best breakdown field intensity of about 90 kV/mm was obtained for 951 tape. The materials 41020 and 951 exhibited the highest volume resistivity. Fabricated devices exhibited safe operation up to a potential difference of 10 kV, limited by minimum clearance. Long-term stability was assured by over 20 kV strength of inner dielectric.
Practical implications
This paper contains description of three devices made in the LTCC technology for application in systems with high-voltage isolation requirement, for example, for power or railway power networks.
Originality/value
The results show that LTCC is a suitable material for fabrication of high-voltage devices with integrated passives. Technology and properties of three examples of such devices are described, demonstrating the ability of the LTCC technology for application in reliable high-voltage devices and systems.
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Beata Barteczka, Piotr Slobodzian, Arkadiusz Dabrowski and Leszek Golonka
The purpose of this paper was to investigate the influence of non-uniform temperature distribution inside a box furnace during the firing process on electrical properties of the…
Abstract
Purpose
The purpose of this paper was to investigate the influence of non-uniform temperature distribution inside a box furnace during the firing process on electrical properties of the low-temperature co-fired ceramic (LTCC) materials used in radio frequency (RF)/microwave applications.
Design/methodology/approach
The authors studied the change in dielectric constant of two popular LTCC materials (DP 951 and DP 9K7) depending on the position of their samples inside the box furnace. Before firing of the samples, temperature distribution inside the box furnace was determined. The dielectric constant was measured using the method of two microstrip lines.
Findings
The findings showed that non-uniform temperature distribution with spatial difference of 6°C can result in 3-4 per cent change of the dielectric constant. It was also found that dielectric constant of the two tested materials shows disparate behavior under the same temperature distribution inside the box furnace.
Practical implications
The dielectric constant of the substrate materials is crucial for RF/microwave applications. Therefore, it was shown that 3-4 per cent deviation in dielectric constant can result in considerable detuning of microwave circuits and antennas.
Originality/value
To the best of the authors’ knowledge, the quantitative description of the impact of temperature distribution inside a box furnace on electrical properties of the LTCC materials has never been published in the open literature. The findings should be helpful when optimizing production process for high yield of reliable LTCC components like filters, baluns and chip antennas.
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Andrzej Dziedzic, Edward Mis, Lars Rebenklau and Klaus‐Jurgen Wolter
This paper aims to present systematic studies of a wide spectrum of geometrical and electrical properties of thick‐film and LTCC microresistors (with designed dimensions between…
Abstract
Purpose
This paper aims to present systematic studies of a wide spectrum of geometrical and electrical properties of thick‐film and LTCC microresistors (with designed dimensions between 50 × 50 μm2 and 800 × 200 μm2).
Design/methodology/approach
The geometrical parameters (average length, width and thickness, relations between designed and real dimensions, distribution of planar dimensions) are correlated with basic electrical properties of resistors (sheet resistance and its distribution, hot temperature coefficient of resistance and its distribution distribution) as well as long term thermal stability and durability of microresistors to short electrical pulses.
Findings
Fodel process gives better resolution than standard screen‐printing and leads to smaller dimensions than designed, smaller absolute error and better uniformity of planar sizes. Microresistors made in full Fodel process show much weaker dimensional effect and exhibit noticeably smaller distribution of basic electrical properties.
Originality/value
Presents systematic studies of a wide spectrum of geometrical and electrical properties of thick‐film and LTCC microresistors.
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Jan Macioszczyk, Karol Malecha and Leszek J. Golonka
The purpose of this paper is a presentation of a miniature vertical dielectric barrier discharge (DBD) plasma generators. The presented devices, with sub- and superstrate, were…
Abstract
Purpose
The purpose of this paper is a presentation of a miniature vertical dielectric barrier discharge (DBD) plasma generators. The presented devices, with sub- and superstrate, were made using low temperature co-fired ceramics (LTCC). Such construction allowed to measure discharge spectra and device temperature easily.
Design/methodology/approach
The generators were made in the Du Pont 951 system with silver vertical metallizations and PdAg contacts. The devices had electrodes with different width and height. Also, the distance between them could be established. They were placed on substrate with buried temperature sensor and covered with a ceramic lid. The lid had opening to measure emitted light. Different configurations of vertical DBD were tested.
Findings
Geometry of vertical metallizations influences on spectra, as well as distance between them. Signal-to-noise ratio had a maximum for certain generators and can be measured by the intensity of highest peak.
Research limitations/implications
Height of vertical metallizations is limited by the difference in shrinkage of LTCC tape and via paste. Parameters of temperature sensors vary between measurements, according to rapid changes of temperature and presence of strong electric field.
Practical implications
The generators can be used for creating discharge for optical emission spectrometry. It is a convenient method to determine the amount of selected gas compounds.
Originality/value
This paper shows fabrication and performance of the novel vertical DBD generators with ceramic additions for convenient spectra measurement and monitoring temperature of the device during work.
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This paper aims to present a method for the reduction of dielectric constant of low-temperature co-fired ceramics (LTCC) substrates with the use of controlled internal porosity.
Abstract
Purpose
This paper aims to present a method for the reduction of dielectric constant of low-temperature co-fired ceramics (LTCC) substrates with the use of controlled internal porosity.
Design/methodology/approach
A glass-ceramic green tape with addition of graphite as a pore former was developed. The green tapes were laminated and then sintered into multilayer structures with porous interior and thin external dense layers. Microstructure of green and fired structures was studied using optical and scanning microscopy. The behavior of the samples during heating was examined in a heating microscope. Impedance spectroscopy was applied for investigation of dielectric properties of the fabricated substrates.
Findings
Microstructure and dielectric properties of the fabricated LTCC structures were compared with the characteristics for non-porous samples with the similar composition. Introduction of 50 Wt.% admixture of graphite in the internal layers of the LTCC substrate was found to result in decrease in dielectric constant value down to about 3. Application of non-porous outer layers improved mechanical strength of the structure and smoothness of its surface, allowing screen printing of conductive pastes on both sides of the substrate.
Practical implications
The rapid growth of the wireless communication industry has created a great demand for the development of new and improved materials and devices operating properly at high frequencies. The fabricated materials can be useful for substrates of microwave devices.
Originality/value
The paper presents an innovative method of dielectric constant decrease of substrate materials. Getting insight into the phenomena responsible for formation of pores is crucial for designing materials for microwave electronics.
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Dominik Jurków and Grzegorz Lis
The purpose of this paper is to present the application of low temperature cofired ceramics (LTCC) technology in the fabrication of a novel electronic device, which consists of an…
Abstract
Purpose
The purpose of this paper is to present the application of low temperature cofired ceramics (LTCC) technology in the fabrication of a novel electronic device, which consists of an antenna amplifier integrated with temperature stabilizer. The temperature controller consists of a thick‐film thermistor and heater, which has been optimized using geometry to achieve uniform temperature distribution on the whole electronic substrate.
Design/methodology/approach
LTCC technology was applied in the fabrication process of the novel device. The temperature distribution on the ceramic substrate and temperature stabilization time were analyzed using an IR camera. The heating ability of the heater was tested in a climatic chamber. The heater and thermistors parameters variability were estimated using a basic mathematical statistic.
Findings
The integrated device ensures proper temperature conditions of electronic components if the ambient temperature is lower than −40°C.
Research limitations/implications
The presented device is just a first prototype. Therefore, the fabrication of the next structures and further experiments will be needed to improve structural drawbacks and to analyze precisely the device reliability and parameters repeatability.
Practical implications
The device presented in the paper can be applied in systems working at very low ambient temperatures (even at −5°C). Moreover, a temperature stabilizer can increase the temperature of the whole device above −40°C, therefore, standard electronic components (which can work down to −40°C) can be used instead of specialized ones (which can work below −40°C).
Originality/value
This paper presents a novel temperature stabilizer.
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Busi Rambabu and Y. Srinivasa Rao
The purpose of this paper is to study high-voltage interactions in polymer thick-film resistors, namely, polyvinyl chloride (PVC)-graphite thick-film resistors, and their…
Abstract
Purpose
The purpose of this paper is to study high-voltage interactions in polymer thick-film resistors, namely, polyvinyl chloride (PVC)-graphite thick-film resistors, and their applications in universal trimming of these resistors.
Design/methodology/approach
The authors applied high voltages in the form of pulses and impulses of various pulse durations and with different amplitudes to polymer thick-film resistors and observed the variation of resistance of these resistors with high voltages.
Findings
The paper finds that high voltages can be used for trimming of polymer thick-film resistors in both directions, i.e. upwards and downwards.
Research limitations/implications
The research implication of this paper is that polymer thick-film resistors can be trimmed downwards or upwards practically using this method.
Practical implications
The practical implications of this paper is that one can trim the polymer thick-film resistors, namely, PVC–graphite thick-film resistors, in both directions, i.e. upwards and downwards, by using this method.
Originality/value
The value of the paper is in showing that high voltages can be used to trim downwards and also upwards in the case of polymer thick-film resistors. This type of trimming is called universal trimming, developed first time for polymer thick-film resistors.
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Darko Belavič, Marko Hrovat, Kostja Makarovič, Gregor Dolanč, Andrej Pohar, Stanko Hočevar and Barbara Malič
– The purpose of this paper is to present the research activity and results to research and development society on the field of ceramic microsystems.
Abstract
Purpose
The purpose of this paper is to present the research activity and results to research and development society on the field of ceramic microsystems.
Design/methodology/approach
The chemical reactor was developed as a non-conventional application of low temperature co-fired ceramic (LTCC) and thick-film technologies. In the ceramic reactor with a large-volume, buried cavity, filled with a catalyst, the reaction between water and methanol produces hydrogen and carbon dioxide (together with traces of carbon monoxide). The LTCC ceramic three-dimensional (3D) structure consists of a reaction chamber, two inlet channels, an inlet mixing channel, an inlet distributor, an outlet collector and an outlet channel. The inlet and outlet fluidic barriers for the catalyst of the reaction chamber are made with two “grid lines”.
Findings
A 3D ceramic structure made by LTCC technology was successfully designed and developed for chemical reactor – methanol decomposition.
Research limitations/implications
Research activity includes the design and the capability of materials and technology (LTCC) to fabricate chemical reactor with large cavity. But further dimensions-scale-up is limited.
Practical implications
The technology for the fabrication of LTCC-based chemical reactor was developed and implemented in system for methanol decomposition.
Originality/value
The approach (large-volume cavity in ceramic structure), which has been developed, can be used for other type of reactors also.
Details
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Darko Belavic, Andraž Bradeško and Hana Uršič
The purpose of this study is to design, fabricate and investigate low-temperature co-fired ceramic (LTCC) structures with integrated microfluidic elements. Special attention is…
Abstract
Purpose
The purpose of this study is to design, fabricate and investigate low-temperature co-fired ceramic (LTCC) structures with integrated microfluidic elements. Special attention is paid to the study of fluid properties of micro-channels and microvalves, which are important constitutive parts of both, microfluidic systems and individual microfluidic devices.
Design/methodology/approach
Several test patterns of fluid channels with different geometry and different types of valves were designed and realized in LTCC technology. All test structures were tested under the flow of two fluids (liquids): water and isopropyl alcohol. Flow rates at different applied pressure were measured and hydrodynamic resistance and diode effect were calculated.
Findings
The investigation of the channels showed that viscosity of fluidic media has significant influence on the hydrodynamic resistance in channels with rectangular cross-section, while this effect is small on channels with square cross-section. The viscosity also has a decisive influence on the diode effect of different shape of valves, and therefore, it is important in the selection of the valve in practical applications.
Research limitations/implications
In this work, the investigation of hydrodynamic resistance of channels and diode effect of passive valves is limited on selected geometry and only on two fluidic media and two applied pressures. All these and some other parameters have a significant influence on fluidic properties, but this will be the topic of the next research work, which will be supported by numerical modelling.
Practical implications
The presented results are useful in the future designing process of LTCC-based microfluidic devices and systems.
Originality/value
Microfluidic in the LTCC structures is an unconventional use of this technology. Therefore, the fluid properties are relatively unsearched. On the other hand, the global use of microfluidic devices and systems is growing rapidly in various applications. They are mostly made by polymer materials, however, in more demanding applications; ceramic is a useful alternative.