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Article
Publication date: 10 June 2020

Camila Fernandes Higa, Thatyanne Gradowski, Selene Elifio-Esposito, Marcelo Fernandes de Oliveira, Paulo Inforçatti, Jorge Vicente Lopes da Silva, Fred Lacerda Amorim and Michelle Sostag Meruvia

This study aims to investigate the production of scaffolds by selective laser sintering (SLS) using poly(vinyl alcohol) (PVA) polymer, for in vitro studies, a relatively new and…

154

Abstract

Purpose

This study aims to investigate the production of scaffolds by selective laser sintering (SLS) using poly(vinyl alcohol) (PVA) polymer, for in vitro studies, a relatively new and growing area in which scaffolds could be used in the design of three-dimensional models for in vitro disease model or tissue equivalent for safety and effectiveness tests.

Design/methodology/approach

The influence of the SLS process parameters laser power, 26 W and 32 W, and number of laser scans, 1, 2, 4 and 6, on the surface microstructure of the samples and on the degree of crystallinity and chemical stability of PVA material, was investigated using powder with particle size of 20-320 µm. Laser sintered PVA samples were subjected to cell culture tests using osteoblastic cells derived from human osteosarcoma (SaOs-2).

Findings

The laser power has no significant influence on the microstructure of the laser-sintered samples, however the number of scans has a considerable influence on the sintering degree; the SLS process causes a decrease in the degree of crystallinity and changes the chemical structure of the as-received PVA, especially when using higher laser power and more number of scans. Preliminary in vitro cell culture tests show that the laser-sintered PVA material is biocompatible with SaOs-2 cells.

Originality/value

SLS offers good potential for the fabrication of scaffolds and thus, may be applied as an alternative to conventional scaffold fabrication processes to overcome their limitations.

Details

Rapid Prototyping Journal, vol. 26 no. 6
Type: Research Article
ISSN: 1355-2546

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Article
Publication date: 21 June 2021

Tiago Czelusniak and Fred Lacerda Amorim

This paper aims to provide a detailed study on influence of the laser energy density on mechanical, surface and dimensional properties of polyamide 12 (PA12) parts produced by…

527

Abstract

Purpose

This paper aims to provide a detailed study on influence of the laser energy density on mechanical, surface and dimensional properties of polyamide 12 (PA12) parts produced by selective laser sintering (SLS), providing the microstructural and crystallization evolution of the samples produced at different energy densities.

Design/methodology/approach

Making use of a space filling design of experiments, a wide range of laser sintering parameters is covered. Surface morphology is assessed by means of profile measurements and scanning electron microscopy (SEM) images. Mechanical testing, SEM, X-ray diffraction (XRD), differential scanning calorimeter (DSC) and infrared spectroscopy (FTIR) were used to assess the influence of energy density on structural and mechanical properties.

Findings

Results show a high dependency of the properties on the laser energy density and also a compromise existing between laser exposure parameters and desired properties of laser sintered parts. Surface roughness could be associated to overlap degree when using higher scan line spacing values and lower laser speeds improved surface roughness when high scan line spacing is used. Higher mechanical properties were found at higher energy density levels, but excessively high energy density decreased mechanical properties. A transition from brittle to ductile fracture with increasing energy density could be clearly observed by mechanical analysis and SEM. XRD and DSC measurements show a decrease on the crystal fraction with increasing energy densities, which corroborated the plastic behavior observed, and FTIR measurements revealed polymer degradation through chain scission might occur at too high energy densities.

Originality/value

Valuable guidelines are given regarding energy density optimization for SLS of PA12 considering not only quality criteria but also microstructure characteristics. Surface properties are studied based on the concept of degree of overlap between laser scanning lines. For the first time, crystallization behavior of SLS PA12 parts produced at different energy levels was studied by means of XRD measurements. Polymer degradation of SLS PA12 parts was evaluated with FTIR, which is a non-destructive and easy test to be conducted.

Details

Rapid Prototyping Journal, vol. 27 no. 6
Type: Research Article
ISSN: 1355-2546

Keywords

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Article
Publication date: 30 September 2013

Fred Lacerda Amorim, Armin Lohrengel, Guenter Schaefer and Tiago Czelusniak

This work aims to investigate the direct production of electrical discharge machining (EDM) electrodes by means of the selective laser sintering (SLS) technique using a new…

422

Abstract

Purpose

This work aims to investigate the direct production of electrical discharge machining (EDM) electrodes by means of the selective laser sintering (SLS) technique using a new non-conventional metal-matrix composite material (TiB2-CuNi). The influence and optimization of the main SLS parameters on the densification behavior and porosity is experimentally studied. EDM experiments are also performed to evaluate the electrodes performance.

Design/methodology/approach

The new EDM electrode material used was a powder system composed of TiB2 and CuNi. Making use of a designed systematic experimental methodology, the effects of layer thickness, laser scan speed and scan line spacing were optimized, where aspects such as densification behavior, porosity and surface morphology of the samples were analyzed through microstructural and surface analysis. EDM experiments were conducted under three different regimes in order to observe the electrodes behavior and performance. The results were compared with copper powder electrodes manufactured by SLS and EDMachined under the same conditions.

Findings

The experimental results showed that the direct SLS manufacturing of composite electrodes is feasible and promising. The laser scan speed has a high effect on the densification behavior of the samples, while the effect of scan line spacing on the porosity is more visible when the overlapping degree is considered. Surface morphology was not affected by the scan line spacing, whereas balling phenomenon was reported, regardless of the scan line spacing. The EDM results showed that the TiB2-CuNi electrodes had a much superior performance than the copper powder electrodes made by SLS, regardless of the EDM regime applied.

Research limitations/implications

Generally, the machine tool itself promotes some restrictions to the SLS process optimization. It is normally attributed to the characteristics of the laser type and the amount of energy that can be delivered to the powder bed. The present investigation could not cover all the optimization potential involved with the studied material due to limitations of the SLS machine tool used.

Originality/value

Significant results on the direct SLS manufacturing of a new non-conventional composite material, which has a great technological potential to be used as an EDM electrode material, are presented. Valuable guidelines are given in regard to the SLS optimization of TiB2-CuNi material and its performance as an EDM electrode. This work also provides a systematic methodology designed to be applied to the SLS process to produce EDM electrodes.

Details

Rapid Prototyping Journal, vol. 19 no. 6
Type: Research Article
ISSN: 1355-2546

Keywords

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