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Article
Publication date: 19 December 2018

Hui Zhang, Yanling Guo, Kaiyi Jiang, David Bourell, Jian Li and Yueqiang Yu

A new kind of polymer mixture (co-PA-PES) was prepared in different mass ratios, by mixing polyether sulfone hot-melt adhesive (PES-HmA) and copolyamide B249 (PA-B249). This study…

Abstract

Purpose

A new kind of polymer mixture (co-PA-PES) was prepared in different mass ratios, by mixing polyether sulfone hot-melt adhesive (PES-HmA) and copolyamide B249 (PA-B249). This study aims to investigate its characteristics of laser sintering and get the optimal process parameters.

Design/methodology/approach

The effect of mass ratio of co-PA-PES on thermal behavior was analyzed using a simultaneous thermal analyzer, and the density and mechanical properties of sintered parts were tested to evaluate the performance of the polymeric system. Scanning electron microscopy and Fourier transform infrared spectroscopy were performed to characterize the microstructure and binding mechanism of sintered co-PA-PES parts. Specifically, mechanical properties of the mixture with 20 Wt.% PA-B249 were optimized based on a design of experiment methodology, along with the restriction of maximum absorbable laser energy density.

Findings

Liquid phase fusion was considered as the main sintering mechanism for co-PA-PES, and mechanical interlocking was the dominant binding mechanism. The effects of mass ratios of this material on the thermal properties, density and mechanical properties were obtained via data results. Additionally, compared to neat PES-HmA, co-20 Wt.% PA-PES showed a 71.7 per cent increase in tensile strength, 24.4 per cent increase in flexural strength and 102.1per cent increase in impact strength.

Originality/value

This paper proposed a new kind of polymer mixture as the feedstock for laser sintering with the advantages of low price and easy processing. The filler of PA-B249 effectively improved the performance of the polymer mixture, including but not limited to mechanical properties.

Details

Rapid Prototyping Journal, vol. 25 no. 3
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 25 July 2019

Hui Zhang, David Bourell, Yanling Guo, Xiaodong Zhang, Yu Zhuang, Yueqiang Yu, Kaiyi Jiang and Wasim M.K. Helal

A pine/co-PES composite (PCPES composite) was proposed as the feedstock for powder bed fusion (laser sintering, LS). This paper aims to provide some necessary experimental data…

Abstract

Purpose

A pine/co-PES composite (PCPES composite) was proposed as the feedstock for powder bed fusion (laser sintering, LS). This paper aims to provide some necessary experimental data and the theoretical foundation for LS of pine/co-PES, especially for the application of using the laser-sintered pine/co-PES parts as complex structural patterns in investment casting.

Design/methodology/approach

The PCPES composites with different pine loadings were mixed mechanically. The composite’s preheating temperature and processing temperature during LS were determined experimentally based on the material’s thermal behavior. The effects of pine powder on the binding mechanism of PCPES composites were discussed through analyzing the microstructure of the laser-sintered parts’. Mechanical properties and dimensional precision of laser-sintered PCPES parts in different pine loadings were tested, and the parts’ mechanical properties were strengthened by wax-infiltration post-processing. The influence extents of process parameters on the mechanical properties of laser-sintered 20 Wt.% pine/co-PES parts were investigated using a 1/2 fractional factorials experiment.

Findings

20 Wt.% pine/co-PES is considered to be a promising wood-plastic composite for laser sintering. The relationship between mechanical strength of its laser-sintered parts and process parameters was built up using mathematical formulas. Experimental results show density, tensile strength, flexural strength and surface roughness of laser-sintered 20 Wt.% pine/co-PES parts are improved by 72.7-75.0%, 21.9-111.3%, 26.8-86.2%, 27.0-29.1% after post-process infiltration with a wax. A promising application of the wax-infiltrated laser-sintered parts is for investment casting cores and patterns.

Research limitations/implications

The proper process parameters and forming properties of laser-sintered parts are limited to the results of laser sintering experiments carried on using AFS 360 rapid prototyping device.

Originality/value

This investigation not only provides a new feedstock for laser sintering with the advantages of low cost and fabricability but also uses an advanced technique to produce personalized wood-plastic parts efficiently. Mathematical models between mechanical properties of laser-sintered PCPES parts and LS process parameters will guide the further LS experiments using the 20 Wt.% pine/co-PES composite. Besides, the laser-sintered PCPES parts after wax-infiltration post-processing are promising as complex structural patterns for use in investment casting.

Details

Rapid Prototyping Journal, vol. 25 no. 8
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 30 May 2008

B. Stevinson, D.L. Bourell and J.J. Beaman

The paper aims to evaluate mechanisms for silicon overfilling including volume expansion of silicon on solidification for composite silicon/silicon carbide (SiC) objects generated…

1098

Abstract

Purpose

The paper aims to evaluate mechanisms for silicon overfilling including volume expansion of silicon on solidification for composite silicon/silicon carbide (SiC) objects generated using post‐process infiltration of selective laser sintered (SLS) SiC preforms.

Design/methodology/approach

Overfilling was characterized through geometrical means and microscopy, and results were used for further study and discussion of overfilling mechanisms.

Findings

Silicon overfilling in silicon infiltrated SLS SiC parts is attributed primarily to its infiltrant silicon volume expansion on solidification. Si/SiC composites were found to be thermally stable with good material bonding.

Research limitations/implications

Silicon as an infiltrant is unusual as it expands on solidification, whereas most infiltrants contract. Overfilling during infiltration of SLS porous performs is therefore not considered to be prevalent.

Originality/value

This paper provides an examination of the value of silicon as an infiltrant material for SLS SiC preforms. Various mechanisms are presented for volume change during post‐process infiltration of indirect SLS non‐metallic performs.

Details

Rapid Prototyping Journal, vol. 14 no. 3
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 14 June 2011

Phani Vallabhajosyula and David L. Bourell

The purpose of this paper is to develop a methodology to achieve successful infiltration of indirect selective laser sintered steel components with ferrous alloys and thereby to…

Abstract

Purpose

The purpose of this paper is to develop a methodology to achieve successful infiltration of indirect selective laser sintered steel components with ferrous alloys and thereby to produce fully ferrous components with desirable properties while preserving part geometry.

Design/methodology/approach

The approach is to generate a “green” part by selective laser sintering (SLS) of ferrous powder mixed with a transient binder in a commercial polymer machine. This part is post‐processed to burn off the transient binder (brown part) and to infiltrate the porous structure with a lower melting point ferrous metal. A critical consideration is loss of part structural integrity by over‐melting after infiltration as a result of chemical diffusion of alloying elements, principally carbon. A predictive model defining the degree of success of infiltration based on chemical equilibrium may be used to select the temperature for infiltration.

Findings

The infiltration temperature should be set such that the equilibrium solid fraction of the final infiltrated part is at least equal to or greater than the brown part solid fraction.

Research limitations/implications

Infiltration temperature must be carefully controlled to prevent melting of the brown part. Effect of alloying elements other than carbon on equilibrium solid fraction is not considered while constructing the predictive model.

Originality/value

This approach can be used to obtain fully ferrous parts with complex geometry and desirable properties using a low‐cost polymer SLS machine.

Details

Rapid Prototyping Journal, vol. 17 no. 4
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 10 June 2021

Anna Liebrich, Horst-Christian Langowski, Regina Schreiber and Bernd R. Pinzer

This study aims to investigate the effect of the material thickness and build orientation on the mass transfer of low molecular weight substances through polyamide 12 (PA12…

87

Abstract

Purpose

This study aims to investigate the effect of the material thickness and build orientation on the mass transfer of low molecular weight substances through polyamide 12 (PA12) structures produced by laser sintering (LS).

Design/methodology/approach

Disc-shaped PA12 sheets having a nominal thickness ranging from 700 to 2,000 µm were built in horizontal, vertical and diagonal orientations and their permeation properties to oxygen and water vapor were measured. The structural properties of the sheets were examined by X-ray micro-computed tomography, differential scanning calorimetry and polarized light microscopy.

Findings

All the LS sheets that were investigated had water vapor and oxygen permeation coefficients that are in the range of those of PA12 produced by traditional manufacturing technologies. Despite significant differences in the porosity characteristics, the permeation properties of sheets built in different orientations were similar. The pores seem to have no measurable effect on the mass transfer rates in the sheets, and the transport processes seem to predominantly follow the rules of a regular solution-diffusion mechanism. The results showed a non-significant trend toward thickness-dependent permeation coefficients, which agrees with the observed differences in the crystal structures of the sheets.

Practical implications

The results are an important basis for the qualification of LS technology for direct manufacturing in applications requiring special barrier performance.

Originality/value

This study provides new information on mechanisms of mass transport through LS PA12 and the effect of the material thickness and build orientation. Furthermore, the results enhance understanding of the structural properties of thin polymeric sheets produced by LS.

Details

Rapid Prototyping Journal, vol. 27 no. 5
Type: Research Article
ISSN: 1355-2546

Keywords

Content available
Book part
Publication date: 26 October 2021

Leandros Savvides

Abstract

Details

3D Printing Cultures, Politics and Hackerspaces
Type: Book
ISBN: 978-1-80071-665-0

Article
Publication date: 26 April 2011

Abhishek Goel and David Bourell

The purpose of this paper is to establish a scientific understanding for electrochemical infiltration of laser sintered (LS) preforms.

Abstract

Purpose

The purpose of this paper is to establish a scientific understanding for electrochemical infiltration of laser sintered (LS) preforms.

Design/methodology/approach

Electrochemical deposition techniques were modified to induce infiltration of nickel ions inside porous LS structures with deposition on pore walls.

Findings

This novel process is feasible and has the potential to produce fully dense parts. Both conductive and non‐conductive preforms can be infiltrated by this method.

Research limitations/implications

Removal of trapped fluids and gases inside the porous structure is one of the major challenges in the described electrochemical infiltration process.

Practical implications

This work enables low‐cost production of structural parts. It expands the application base for additive manufacturing, especially laser sintering technology.

Social implications

The novel process carried out in this research is energy efficient when compared to state‐of‐the‐art vacuum‐melt infiltration.

Originality/value

The proposed process is a novel method for facilitating room‐temperature infiltration of porous LS preforms.

Details

Rapid Prototyping Journal, vol. 17 no. 3
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 12 March 2020

Shekhar Srivastava, Rajiv Kumar Garg, Vishal S. Sharma, Noe Gaudencio Alba-Baena, Anish Sachdeva, Ramesh Chand and Sehijpal Singh

This paper aims to present a systematic approach in the literature survey related to metal additive manufacturing (AM) processes and its multi-physics continuum modelling approach…

Abstract

Purpose

This paper aims to present a systematic approach in the literature survey related to metal additive manufacturing (AM) processes and its multi-physics continuum modelling approach for its better understanding.

Design/methodology/approach

A systematic review of the literature available in the area of continuum modelling practices adopted for the powder bed fusion (PBF) AM processes for the deposition of powder layer over the substrate along with quantification of residual stress and distortion. Discrete element method (DEM) and finite element method (FEM) approaches have been reviewed for the deposition of powder layer and thermo-mechanical modelling, respectively. Further, thermo-mechanical modelling adopted for the PBF AM process have been discussed in detail with its constituents. Finally, on the basis of prediction through thermo-mechanical models and experimental validation, distortion mitigation/minimisation techniques applied in PBF AM processes have been reviewed to provide a future direction in the field.

Findings

The findings of this paper are the future directions for the implementation and modification of the continuum modelling approaches applied to PBF AM processes. On the basis of the extensive review in the domain, gaps are recommended for future work for the betterment of modelling approach.

Research limitations/implications

This paper is limited to review only the modelling approach adopted by the PBF AM processes, i.e. modelling techniques (DEM approach) used for the deposition of powder layer and macro-models at process scale for the prediction of residual stress and distortion in the component. Modelling of microstructure and grain growth has not been included in this paper.

Originality/value

This paper presents an extensive review of the FEM approach adopted for the prediction of residual stress and distortion in the PBF AM processes which sets the platform for the development of distortion mitigation techniques. An extensive review of distortion mitigation techniques has been presented in the last section of the paper, which has not been reviewed yet.

Article
Publication date: 1 March 1995

Mukesh Agarwala, David Bourell, Joseph Beaman, Harris Marcus and Joel Barlow

Considers efforts to date to produce parts by direct selective laser sintering (SLS) of metals, including post processing to improve structural integrity and/or to induce a…

13342

Abstract

Considers efforts to date to produce parts by direct selective laser sintering (SLS) of metals, including post processing to improve structural integrity and/or to induce a transformation. Provides a brief overview of the basic principles of SLS machine operation, and discusses materials issues affecting direct SLS of metals and the resultant properties and microstructures of the parts. Reviews results of past efforts on SLS of metal systems such as Cu‐Sn, Cu‐Solder (Pb‐Sn), Ni‐Sn, pre‐alloyed bronze (Cu‐Sn). Finally discusses more recent efforts on SLS of bronze‐nickel powder mixtures in greater detail.

Details

Rapid Prototyping Journal, vol. 1 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 18 April 2016

Jan Patrick Deckers, Khuram Shahzad, Ludwig Cardon, Marleen Rombouts, Jozef Vleugels and Jean-Pierre Kruth

The purpose of this paper is to compare different powder metallurgy (PM) processes to produce ceramic parts through additive manufacturing (AM). This creates the potential to…

Abstract

Purpose

The purpose of this paper is to compare different powder metallurgy (PM) processes to produce ceramic parts through additive manufacturing (AM). This creates the potential to rapidly shape ceramic parts with an almost unlimited shape freedom. In this paper, alumina (Al2O3) parts are produced, as Al2O3 is currently the most commonly used ceramic material for technical applications.

Design/methodology/approach

Variants of the following PM route, with indirect selective laser sintering (indirect SLS) as the AM shaping step, are explored to produce ceramic parts: powder synthesis, indirect SLS, binder removal and furnace sintering and alternative densification steps.

Findings

Freeform-shaped Al2O3 parts with densities up to approximately 90 per cent are obtained.

Research limitations/implications

The resulting Al2O3 parts contain inter-agglomerate pores. To produce higher-quality ceramic parts through indirect SLS, these pores should be avoided or eliminated.

Originality/value

The research is innovative in many ways. First, composite powders are produced using different powder production methods, such as temperature-induced phase separation and dispersion polymerization. Second, four different binder materials are investigated: polyamide (nylon-12), polystyrene, polypropylene and a carnauba wax – low-density polyethylene combination. Further, to produce ceramic parts with increased density, the following densification techniques are investigated as additional steps of the PM process: laser remelting, isostatic pressing and infiltration.

Details

Rapid Prototyping Journal, vol. 22 no. 3
Type: Research Article
ISSN: 1355-2546

Keywords

1 – 10 of 315