Functionally Nb graded inconel 718 alloys fabricated by laser melting deposition: mechanical properties and corrosion behavior

Abstract

Purpose

Laser melting deposition (LMD) is an advanced additive manufacturing (AM) technology without powder waste, and nickel-based alloys with different Nb contents were created one-time by adjusting the ratio of mixed powders via a dual-feed system. Here, the authors provide a systematic report on the effects of the Nb content on the microstructure, Laves phase segregation and mechanical properties of as-received LMD nickel-based alloys. The effects of the Nb content on the microstructure, precipitation evolution and mechanical properties of the subsequent heat-treated LMD samples are also discussed in this paper.

Design/methodology/approach

Thus, the present research aims to obtain a better understanding of the effect of Nb content on the microstructural and mechanical properties of the as-received LMD Inconel 718 alloys through high-throughput sample fabrication. The microstructures were characterized by scanning electron microscopy and energy-dispersive spectroscopy, electron back-scattered diffraction and transmission electron microscopy methods. The mechanical properties were obtained from compressive tests and nano-indentation tests. Electrochemical tests, including electrochemical impedance spectroscopy and potentiodynamic polarizations, were carried out to evaluate the durability of the Inconel 718 alloys. Results can provide a factual basis for future applications of the functionally graded by AM technology.

Findings

The grain size of the as-received LMD Inconel 718 alloys decreased with the Nb content. The Laves phase distribution at the macro level was relatively uniform and the Laves phase exhibited a 1.5-fold nano-hardness compared with the matrix. The strength improvement for the as-received LMD Inconel 718 alloys with Nb content was attributed to grain refinement and enhancement of the Laves phase in terms of both hardness and content. Meanwhile, the corrosion resistance increased with the increase of the Nb content, especially for the pitting potential, which was attributed to the optimization of carbide precipitates due to the strong affinity between niobium and carbon.

Originality/value

The results provide a factual basis for the Nb content effect in LMD nickel-based alloys, and this method can greatly promote the development of new materials. The authors believe that this study makes a significant contribution to the literature and is suitable for publication.

Citation

Ni, X., Zhang, L., Wu, W., Zhu, D., Kong, D., Dong, C. and Zhu, G. (2020), "Functionally Nb graded inconel 718 alloys fabricated by laser melting deposition: mechanical properties and corrosion behavior", Anti-Corrosion Methods and Materials, Vol. 67 No. 1, pp. 16-23. https://doi.org/10.1108/ACMM-06-2019-2131